中国科学技术大学学报 ›› 2011, Vol. 41 ›› Issue (5): 432-438.DOI: 10.3969/j.issn.0253-2778.2011.05.009

• 原创论文 • 上一篇    下一篇

黏弹性材料纳米压痕测试及接触形貌的影响

洪 磊   

  1. 1.安徽大学电气工程与自动化学院,安徽合肥 230039; 2.中国科学技术大学工程与材料科学实验中心,安徽合肥 230026; 3.中国科学技术大学精密机械与精密仪器系,安徽合肥 230026
  • 收稿日期:2011-01-05 修回日期:2011-05-03 出版日期:2011-05-31 发布日期:2011-05-31
  • 通讯作者: 苏亚辉
  • 作者简介:洪磊,男,1988年生,硕士生. 研究方向:微机电系统. E-mail: hongmaolei@yahoo.cn
  • 基金资助:
    国家自然科学基金(50275140,50335050),安徽大学人才队伍建设经费资助.

Nano-indentation test of visco-elastic materials and the influence of contact geometry on indentation

HONG Lei   

  1. 1.College of Electrical Engineering and Automation, AHU, Hefei 230039, China; 2.Materials Science and Engineering Testing Center, USTC, Hefei 230026, China; 3.Precision Machinery and Precision Instrument Department, USTC, Hefei 230026, China
  • Received:2011-01-05 Revised:2011-05-03 Online:2011-05-31 Published:2011-05-31

摘要: 利用纳米硬度计测量聚氯乙烯(PVC)的力学性能,用有限元软件仿真了实测过程,比对实验和仿真数据,得出有限元法研究黏弹性材料纳米压痕实验的可行性结论.据此针对不同尖端曲率半径的圆锥形压头,模拟纳米压痕测量过程,结果显示:在黏弹性材料纳米压痕实验中硬度测量值随压入深度的增加而减小,随尖端曲率半径的增加而增大.最后引入压头表征尺寸概念,针对表征尺寸与表面粗糙度参数在同一数量级以及表征尺寸远小于表面粗糙度参数这两种情况分别进行仿真,结果表明:接触零点在峰顶或谷底时的硬度测量值会相应地偏小或偏大,并且硬度测量值的偏差随纹波间距和轮廓最大高度的增加而增大.

关键词: 黏弹性, 纳米压痕, 有限元, 尖端曲率半径, 粗糙度

Abstract: Instrumented nano-indentation was performed on polyvinyl chloride (PVC) material and finite element method (FEM) calculation was used to simulate the nano-indentation experiment. The data of the FEM calculation and nano-indentation experiment were compared. It was concluded that the method of using FEM to simulate experiments of nano-indentation into visco-elastic materials is feasible. Four 2D axisymmetric FEM modules of conical-indenters with different tip radii were built to interact with PVC. The simulation results show that the measured hardness increases with the tip radius and decreases with the depth of indention in nano-indentation of visco-elastic materials. Indenter dimension index was employed to help establish two FEM modules classified by the difference between the indenter dimension index and surface roughness. The simulation results indicate that the measured hardness is under or over the proper value when the point of surface contact is at its maximum or minimum and that the deviation of hardness increases with that of roughness as well as the distance between the ripples.

Key words: visco-elasticity, nano-indentation, finite element method, tip radius, roughness